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Methods
Describe validated analytical procedures, including LC–MS/MS conditions, sample preparation, calibration, and data analysis.
Raw-data records
Maintain chromatograms, mass spectra, peak information, instrument files, and sample results.
Developing a Documentation System
A documentation system is a structured way to create, organize, control, and store all laboratory documents so that work can be performed consistently and results can be easily traced. For an LC–MS/MS laboratory,
SOPs
SOPs – Provide step-by-step instructions for routine activities such as instrument operation, maintenance, and sample preparation.
Protocols
Describe specific experimental procedures and study plans.
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